Synthesis and characterization of magnetic iron oxide nanoparticles

Lingyan Wang; Jin Luo; Mathew M. Maye; Quan Fan; Qiang Rendeng; Jian Q. Wang; Mark H. Engelhard; Chongmin Wang; Yuehe Lin; Eric I. Altman; Chuan Jian Zhong

doi:10.1557/proc-853-i4.12

Synthesis and characterization of magnetic iron oxide nanoparticles

Lingyan Wang, Jin Luo, Mathew M. Maye, Quan Fan, Qiang Rendeng, Jian Q. Wang, Mark H. Engelhard, Chongmin Wang, Yuehe Lin, Eric I. Altman, Chuan Jian Zhong

Research output: Chapter in Book/Entry/Poem › Conference contribution

1 Scopus citations

Abstract

This paper describes the results of an investigation of modified synthetic protocols to produce monodispersed magnetic ferrite nanoparticles, γ-Fe₂O₃ and Fe₃O₄, and their magnetic properties. The synthesis involved thermal decomposition of organometallic precursors followed by oxidation or reduction. In the synthesis of γ-Fe₂O₃, iron pentacarbonyl was used as the precursor and trimethylamine oxide as the oxidant. In the synthesis of Fe ₃O₄, iron (III) acetylacetonate was reduced by 1,2-hexadecanediol. The particle sizes ranged from 5-15 nm with high monodispersity. Results from TEM, XPS, and SQUID characterizations of these iron oxide nanoparticles are discussed.

Original language	English (US)
Title of host publication	Fabrication and New Applications of Nanomagnetic Structures
Publisher	Materials Research Society
Pages	9-14
Number of pages	6
ISBN (Print)	1558998055, 9781558998056
DOIs	https://doi.org/10.1557/proc-853-i4.12
State	Published - 2004
Externally published	Yes
Event	2004 MRS Fall Meeting - Boston, MA, United States Duration: Nov 29 2004 → Dec 3 2004

Publication series

Name	Materials Research Society Symposium Proceedings
Volume	853
ISSN (Print)	0272-9172

Other

Other	2004 MRS Fall Meeting
Country/Territory	United States
City	Boston, MA
Period	11/29/04 → 12/3/04

ASJC Scopus subject areas

General Materials Science
Condensed Matter Physics
Mechanics of Materials
Mechanical Engineering

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10.1557/proc-853-i4.12

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Wang, L., Luo, J., Maye, M. M., Fan, Q., Rendeng, Q., Wang, J. Q., Engelhard, M. H., Wang, C., Lin, Y., Altman, E. I., & Zhong, C. J. (2004). Synthesis and characterization of magnetic iron oxide nanoparticles. In Fabrication and New Applications of Nanomagnetic Structures (pp. 9-14). (Materials Research Society Symposium Proceedings; Vol. 853). Materials Research Society. https://doi.org/10.1557/proc-853-i4.12

Wang, L, Luo, J, Maye, MM, Fan, Q, Rendeng, Q, Wang, JQ, Engelhard, MH, Wang, C, Lin, Y, Altman, EI & Zhong, CJ 2004, Synthesis and characterization of magnetic iron oxide nanoparticles. in Fabrication and New Applications of Nanomagnetic Structures. Materials Research Society Symposium Proceedings, vol. 853, Materials Research Society, pp. 9-14, 2004 MRS Fall Meeting, Boston, MA, United States, 11/29/04. https://doi.org/10.1557/proc-853-i4.12

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title = "Synthesis and characterization of magnetic iron oxide nanoparticles",

abstract = "This paper describes the results of an investigation of modified synthetic protocols to produce monodispersed magnetic ferrite nanoparticles, γ-Fe2O3 and Fe3O4, and their magnetic properties. The synthesis involved thermal decomposition of organometallic precursors followed by oxidation or reduction. In the synthesis of γ-Fe2O3, iron pentacarbonyl was used as the precursor and trimethylamine oxide as the oxidant. In the synthesis of Fe 3O4, iron (III) acetylacetonate was reduced by 1,2-hexadecanediol. The particle sizes ranged from 5-15 nm with high monodispersity. Results from TEM, XPS, and SQUID characterizations of these iron oxide nanoparticles are discussed.",

author = "Lingyan Wang and Jin Luo and Maye, {Mathew M.} and Quan Fan and Qiang Rendeng and Wang, {Jian Q.} and Engelhard, {Mark H.} and Chongmin Wang and Yuehe Lin and Altman, {Eric I.} and Zhong, {Chuan Jian}",

year = "2004",

doi = "10.1557/proc-853-i4.12",

language = "English (US)",

isbn = "1558998055",

series = "Materials Research Society Symposium Proceedings",

publisher = "Materials Research Society",

pages = "9--14",

booktitle = "Fabrication and New Applications of Nanomagnetic Structures",

note = "2004 MRS Fall Meeting ; Conference date: 29-11-2004 Through 03-12-2004",

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TY - GEN

T1 - Synthesis and characterization of magnetic iron oxide nanoparticles

AU - Wang, Lingyan

AU - Luo, Jin

AU - Maye, Mathew M.

AU - Fan, Quan

AU - Rendeng, Qiang

AU - Wang, Jian Q.

AU - Engelhard, Mark H.

AU - Wang, Chongmin

AU - Lin, Yuehe

AU - Altman, Eric I.

AU - Zhong, Chuan Jian

PY - 2004

Y1 - 2004

N2 - This paper describes the results of an investigation of modified synthetic protocols to produce monodispersed magnetic ferrite nanoparticles, γ-Fe2O3 and Fe3O4, and their magnetic properties. The synthesis involved thermal decomposition of organometallic precursors followed by oxidation or reduction. In the synthesis of γ-Fe2O3, iron pentacarbonyl was used as the precursor and trimethylamine oxide as the oxidant. In the synthesis of Fe 3O4, iron (III) acetylacetonate was reduced by 1,2-hexadecanediol. The particle sizes ranged from 5-15 nm with high monodispersity. Results from TEM, XPS, and SQUID characterizations of these iron oxide nanoparticles are discussed.

AB - This paper describes the results of an investigation of modified synthetic protocols to produce monodispersed magnetic ferrite nanoparticles, γ-Fe2O3 and Fe3O4, and their magnetic properties. The synthesis involved thermal decomposition of organometallic precursors followed by oxidation or reduction. In the synthesis of γ-Fe2O3, iron pentacarbonyl was used as the precursor and trimethylamine oxide as the oxidant. In the synthesis of Fe 3O4, iron (III) acetylacetonate was reduced by 1,2-hexadecanediol. The particle sizes ranged from 5-15 nm with high monodispersity. Results from TEM, XPS, and SQUID characterizations of these iron oxide nanoparticles are discussed.

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UR - http://www.scopus.com/inward/citedby.url?scp=34249897756&partnerID=8YFLogxK

U2 - 10.1557/proc-853-i4.12

DO - 10.1557/proc-853-i4.12

M3 - Conference contribution

AN - SCOPUS:34249897756

SN - 1558998055

SN - 9781558998056

T3 - Materials Research Society Symposium Proceedings

SP - 9

EP - 14

BT - Fabrication and New Applications of Nanomagnetic Structures

PB - Materials Research Society

T2 - 2004 MRS Fall Meeting

Y2 - 29 November 2004 through 3 December 2004

ER -

Synthesis and characterization of magnetic iron oxide nanoparticles

Abstract

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