Hydrothermal synthesis and crystal and molecular structure of a reduced, arsenic rich heteropolyanion, Na4[Mo4As6O 20(OH)2]·9H2O

M. Ishaque Khan, Qin Chen, Jon A Zubieta

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Abstract

The hydrothermal reaction of Na3MoO4·2H 2O, Mo metal, MnO3, H5As3O 10, NaCl and H2O in the mole ratio 6: 6: 6: 3: 10: 166 for 110 h at 180°C yielded orange crystals of the sodium salt of the arsenic-rich MoV-AsIII polyanion cluster, Na 4[Mo4As6O20(OH)2] ·9H2O.

Original languageEnglish (US)
Pages (from-to)356-357
Number of pages2
JournalJournal of the Chemical Society, Chemical Communications
Issue number4
DOIs
StatePublished - 1993

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ASJC Scopus subject areas

  • Molecular Medicine

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