Crystal engineering of inorganic/organic composite solids: The structure-directing role of aromatic ammonium cations in the synthesis of the 'step'-layered molybdenum oxide phase [4,4′-H2bpy][Mo7O22]·H 2O

Pamela J. Zapf; Robert C. Haushalter; Jon Zubieta

doi:10.1039/a607022a

Crystal engineering of inorganic/organic composite solids: The structure-directing role of aromatic ammonium cations in the synthesis of the 'step'-layered molybdenum oxide phase [4,4′-H₂bpy][Mo₇O₂₂]·H ₂O

Pamela J. Zapf, Robert C. Haushalter, Jon Zubieta

Department of Chemistry

Research output: Contribution to journal › Article › peer-review

122 Scopus citations

Abstract

The hydrothermal reaction of MoO₃, Mo metal, NiCl₂ and 4,4′-bipyridine yields a step-layered molybdenum oxide [4,4′-H₂bpy)][Mo₇O₂₂]·H ₂O, a material structurally related to layered MoO₃.

Original language	English (US)
Pages (from-to)	321-322
Number of pages	2
Journal	Chemical Communications
Issue number	3
DOIs	https://doi.org/10.1039/a607022a
State	Published - 1997

ASJC Scopus subject areas

Catalysis
Electronic, Optical and Magnetic Materials
Ceramics and Composites
General Chemistry
Surfaces, Coatings and Films
Metals and Alloys
Materials Chemistry

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Crystal engineering of inorganic/organic composite solids: The structure-directing role of aromatic ammonium cations in the synthesis of the 'step'-layered molybdenum oxide phase [4,4′-H₂bpy][Mo₇O₂₂]·H ₂O. / Zapf, Pamela J.; Haushalter, Robert C.; Zubieta, Jon.
In: Chemical Communications, No. 3, 1997, p. 321-322.

Research output: Contribution to journal › Article › peer-review

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abstract = "The hydrothermal reaction of MoO3, Mo metal, NiCl2 and 4,4′-bipyridine yields a step-layered molybdenum oxide [4,4′-H2bpy)][Mo7O22]·H 2O, a material structurally related to layered MoO3.",

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